气相色谱法检测无水肼中水含量的不确定度评定

对气相色谱法检测无水肼中水含量过程的不确定度进行评定,系统分析检测过程中不确定度来源和各不确定度分量对分析结果的影响,通过对不确定度的分量进行分析和合成,可知标准溶液配制的过程、标准曲线的拟合和测量样品时的重复操作带来的不确定度分量是影响无水肼中水含量测定不确定度的主要来源.     

Response of the EIA ionosphere to the 7-8 May 2005 geomagnetic storm

In this paper, response of low latitude ionosphere to a moderate geomagnetic storm of 7–8 May 2005 (SSC: 1920 UT on 7 May with Sym-H minimum, ∼−112 nT around 1600 UT on 8 May) has been investigated using the GPS measurements from a near EIA crest region, Rajkot (Geog. 22.29°N, 70.74°E, Geomag.14°), India. We found a decrease in total electron content (TEC) in 12 h after the onset of the storm, an increase during and after 6 h of Sym-H deep minimum with a decrease below its usual-day level on the second day during the recovery phase of the storm. On 8 May, an increase of TEC is observed after sunset and during post-midnight hours (maximum up to 170%) with the formation of ionospheric plasma bubbles followed by a nearly simultaneous onset of scintillations at L-band frequencies following the time of rapid decrease in Sym-H index (−30 nT/h around 1300 UT).     

A nonlinear background removal method for seismo-ionospheric anomaly analysis under a complex solar activity scenario: A case study of the M9.0 Tohoku earthquake

A precise determination of ionospheric total electron content (TEC) anomaly variations that are likely associated with large earthquakes as observed by global positioning system (GPS) requires the elimination of the ionospheric effect from irregular solar electromagnetic radiation. In particular, revealing the seismo-ionospheric anomalies when earthquakes occurred during periods of high solar activity is of utmost importance. To overcome this constraint, a multiresolution time series processing technique based on wavelet transform applicable to global ionosphere map (GIM) TEC data was used to remove the nonlinear effect from solar radiation for the earthquake that struck Tohoku, Japan, on 11 March, 2011. As a result, it was found that the extracted TEC have a good correlation with the measured solar extreme ultraviolet flux in 26–34 nm (EUV_26–34) and the 10.7 cm solar radio flux (F_10.7). After removing the influence of solar radiation origin in GIM TEC, the analysis results show that the TEC around the forthcoming epicenter and its conjugate were significantly enhanced in the afternoon period of 8 March 2011, 3 days before the earthquake. The spatial distributions of the TEC anomalous and extreme enhancements indicate that the earthquake preparation process had brought with a TEC anomaly area of size approximately 1650 and 5700 km in the latitudinal and longitudinal directions, respectively.     

Solar activity dependence of total electron content derived from GPS observations over Mbarara

Vertical total electron content (VTEC) observed at Mbarara (geographic co-ordinates: 0.60°S, 30.74°E; geomagnetic coordinates: 10.22°S, 102.36°E), Uganda, for the period 2001–2009 have been used to study the diurnal, seasonal and solar activity variations. The daily values of the 10.7 cm radio flux (F_10.7) and sunspot number (R) were used to represent Solar Extreme Ultraviolet Variability (EUV). VTEC is generally higher during high solar activity period for all the seasons and increases from 0600 h LT and reaches its maximum value within 1400 h–1500 h LT. All analysed linear and quadratic fits demonstrate positive VTEC-F_10.7 and positive VTEC-R correlation, with all fits at 0000 h and 1400 h LT being significant with a confidence level of 95% when both linear and quadratic models are used. All the fits at 0600 h LT are insignificant with a confidence level of 95%. Generally, over Mbarara, quadratic fit shows that VTEC saturates during all seasons for F_10.7 more than 200 units and R more than 150 units. The result of this study can be used to improve the International Reference Ionosphere (IRI) prediction of TEC around the equatorial region of the African sector.     

纳米铝粉的活性评价方法研究进展

综述了纳米铝粉活性的2类评价方法:单质铝含量法和热分析参数法.单质铝含量的测定方法主要有气体容量法、氧化还原滴定法、热重分析法和透射电镜分析法,其中氧化还原滴定法又可分为重铬酸钾滴定法、水溶剂高锰酸钾滴定法、非水溶剂高锰酸钾滴定法及硫酸高铈法.基于热分析参数的活性评价方法主要采用:氧化起始温度、最大氧化速率、一定温度范...     

电机生产企业绿色工厂评价内容、指标及方法的研究

为积极响应《中国制造2025》以及《工业和信息化部办公厅关于开展绿色制造体系建设的通知》,针对我国目前在电机生产行业相关绿色工厂评价要求缺失的现状,结合我国电机生产企业的物料使用特点、生产工艺特点、生产装备特点、产品特点、能源利用特点、主要污染物排放特点等6个方面,对电机生产企业绿色工厂评价内容、指标及方法进行研究。该研究为我国电机生产行业全面推行绿色制造,加快电机生产行业绿色改造升级,构建电机生产行业绿色制造体系,提高我国电机生产行业的国际竞争力作出积极贡献。     

单晶合金蠕变性能影响因素分析

通过分析热处理工艺、元素含量、晶体取向性以及温度和应力对蠕变性能的影响,得出任何1种影响合金蠕变性能的因素其实质都是改变了合金的微观组织,并最终反映到γ′筏形的完善程度S、终端密度TD和线性密度LD上。S值越接近1,γ′筏形的完善程度越好,蠕变寿命就越长;而TD和LD值越大,微观组织图内筏形交叉和中断的数目就越多,蠕变寿命就越短。     

基于模板匹配整帧屏幕视频帧内无损编码方法

当前主流的视频压缩标准,如H.264、HEVC等,主要是针对摄像机拍摄的视频而设计的.而屏幕内容(SC)的视频是由计算机生成的,无噪声,要求更高的压缩效率,同时与摄像机拍摄的视频相比包含更多的结构相似性.提出了一种利用屏幕视频中相似性的模板匹配帧内编码方法,采用由21个像素点组成的模板,以像素点为最小单位对整帧进行模板匹配,并使用哈希函数实现高效的模板查找,最后对残差图像进行熵编码.实验结果显示,与标准的HEVC扩展方法相比,该方法在无损编码上压缩率可以提高一倍,编码时间减小了近一半.      

压辊材料及形状对纤维铺放压紧效果的影响

近年来纤维铺放（AFP）技术被广泛用于大型复杂飞机复合材料构件成型。为了保证纤维铺放过程的一致性,纤维铺放压辊必须在适应芯模型面的同时具有较好的压紧力分布均匀性。鉴于此,对不同弹性模量的压辊材料进行了试验分析,薄膜压力传感器及超声显微镜测试结果表明,低弹性模量的压辊材料变形较大,较好地适应了芯模表面,压力分布相对均匀且可以减少铺层的层间孔隙数量,硅橡胶压辊比聚乙烯压辊压紧力分布均匀性提高了50%~60%,铺层孔隙率降低了92.1%。针对孔隙分布主要集中在压辊两端及压紧力在压辊两端下降幅度较大的问题,采用ANSYS Workbench对压辊端部进行斜端面优化,得到最优倾斜角度为20°;测试结果表明斜端面压辊压力分布均匀性比直断面压辊提高了42.9%,铺层孔隙率下降了51.6%。     

基于Web信息处理的机位信息融合设计与实现

基于Web应用逆向工程提出一种网页信息提取的数据融合方案,利用HTTP的POST请求智能获取网页信息,通过自定义串口协议将数据送至服务器,最终采用C#正则表达式提取有效信息,设计在汕头空管站飞行计划处理系统(FIPS)与潮汕机场航班信息查询系统的数据融合中投入实际应用。